It is obtained by condensation of triethyl orthoformate and glacial acetic acid by ammonia. Triethyl orthoformate was added to glacial acetic acid for heating, and reacted with ammonia for 1.5 h to precipitate white crystals, and then continue to pass ammonia for half an hour. The reactant was subjected to atmospheric distillation first, and then the alcohol was distilled off under reduced pressure and reduced pressure. Cold to 25 ° C, washed with anhydrous ethanol, filtered, dried to give methyl acetate.
More About Formamidine acetate：
CAS NO: 3473-63-0
Molecular formula: C3H8N2O2
Melting point: 158-161 °C (dec.)(lit.)
|Loss on drying||0.5%max|
Use Of Formamidine acetate:
Formamidine acetate is mainly used for the synthesis of a class of biologically active compounds such as the antitumor drug 4-hydroxy-5-fluoropyrimidine, and also for the synthesis of cyclohexapeptide antifungal drugs, synthesis of trichloropyrimidine, etc.
Package Of Formamidine acetate:
Storage:Stored in a closed, low temperature, heated to decompose into ammonia and acetic acid